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Title
Hydrate cellulose films and preparation of samples modified with nickel nano- and microparticles. II. Intercalation of nickel into hydrate cellulose films
Authors
NINA E. KOTELNIKOVA and ALEXANDRA M. MIKHAILIDI
Received
March 22, 2011
Published
Volume 46 Issue 1-2 January-February
Keywords
hydrate cellulose film, nickel nano- and microparticles, X-ray diffraction, SEM analysis
Abstract
Nanocomposite materials containing stabilized nickel nano- and microparticles in the matrix of the hydrate cellulose film (HCF) have been prepared. Ni nanoparticles were synthesized directly in the film, by the diffusion-reduction method. The efficiency of reducers on the chemical reduction of nickel ions has been compared. The crystalline structure of the HCF-Ni samples was analyzed by X-ray diffraction, and their morphology was studied by SEM analysis. The structure of the cellulose remained unchanged was compared to the pristine one. Particle sizes, dependent on the reducer type, were measured in nanometers, according to the micrometer scale.
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