Cellulose Chemistry and Technology

ADVANCES IN THE CHEMISTRY, PHYSICS AND TECHNOLOGY
OF PULP, PAPER AND CELLULOSE-BASED MATERIALS

ISSN 2457-9459 (Online)
ISSN-L 0576-9787 (Print)


2023

Journal Citation Reports
Impact factor 2023: 1.3
5-Year Impact Factor: 1.2
Article Influence® Score: 0.140
Ranked 9 out of 23
MATERIALS SCIENCE, PAPER & WOOD (Q2)

Scopus
CiteScore 2023: 2.3
SNIP: 0.405

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SJR: 0.264
H-Index: 42
Ranked Q3

 

Title
Effects of acid hydrolysis time on cellulose nanocrystals properties: Nanoindentation and thermogravimetric studies
Authors
P. KRISHNAMACHARI R. HASHAIKEH M. CHIESA and K. R. M. GAD EL RAB

Received April 27, 2011
Published Volume 46 Issue 1-2 January-February
Keywords nanocellulose, nanoindentation, acid hydrolysis, thermal analysis

Abstract
Nanoindentation and thermogravimetric studies were performed on different samples obtained from acid hydrolysis of Microcrystalline Cellulose (MCC). Acid hydrolysis of MCC was carried out using 64% HSO at 45 °C for 10, 20, 30 2 4 min, 1 and 5 h, respectively. Elastic modulus and hardness were assessed for each sample. The samples hydrolyzed for 30 min or more had a considerably lower elastic modulus than those hydrolyzed for 20 min or less. Thermogravimetric (TGA) studies revealed that the onset of thermal degradation of all samples occurred at a lower temperature than that of MCC.


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